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Versatile Spectrometer suits Diamond Light Source
Versatile Spectrometer Suits Diamond Light Source When the Microfocus Spectroscopy beamline of Diamond Light Source discovered a need to scan initial mineral samples to highlight areas within the samples for the synchrotron light, they turned to Fischer Instrumentation (GB) Ltd, specialists in x-ray material analysis. Diamond Light Source is based on the Harwell Science and Innovation Campus near Didcot, Oxfordshire and from here it uses electrons to produce x-ray, infrared and ultra-violet beams of exceptional brightness, known as synchrotron light. From these highly focused beams of light, scientists and engineers are able to probe deep into the basic structure of matter and materials at the atomic and molecular level to lead scientific breakthroughs in the fields of biotechnology, medicine, environmental and materials science. There are currently nine operational experimental stations or beamlines within Diamond, with 13 more due for completion by 2012, and the Microfocus Spectroscopy beamline is world class in the mapping of inhomogeneous mineral samples under Principal Beamline Scientist Dr Fred Mosselmans. Mineral samples are understood to have varying compositions and the Fischer XDAL Spectrometer system was selected with its beam of 100 microns diameter to scan initial mineral samples and highlight the areas within the samples for the synchrotron light, with its highly focused beam of about 2 micron diameter. “The Fischer XDAL spectrometer was chosen for the task because of its ability to cover a wide range of elements and its cost-effectiveness” comments Principal Beamline Scientist, Dr Fred Mosselmans. X-Ray fluorescence is a highly effective tool for materials analysis. It is widely used for coating thickness measurement and is also well suited for element identification as this case proves. The samples can be evaluated in almost any dimension and condition. Powder and paste can be analyzed in the same manner as solid materials or liquids. The X-Ray XAN and XDAL are energy dispersive high-performance X-Ray fluorescence spectrometer systems, which provide simple, fast and accurate analysis of unknown materials. Element detection from Aluminum to Uranium is possible even at very low concentrations. The exceptionally powerful capabilities of these unique instruments are achieved by the use of a semiconductor detector with Peltier cooling for high spectral energy resolution and the WinFTM® Version 6 Software for materials and multi-dimensional coating analysis. The Diamond Light Source beamline project is another example of how versatile the Fischer spectrometer systems are and how diverse the applications can be. Take, for example, the 15 Fischer spectrometer systems providing a cost efficient service for Assay Offices across the UK and Europe. This is because, when used in combination with the application kit Gold Assay, these instruments are suited for the fast, non-destructive and accurate gold content measurement in jewelry and precious metals. Ray Scruby, MD of Fischer Instrumentation (GB) Ltd comments on the latest high profile contract for Fischer : “We are proud to be associated with the pioneering research of the Diamond Light Source and our long-standing reputation for well made materials analysis instrumentation manufactured by Helmut-Fischer GmbH will ensure reliability and longevity for the Diamond project”. The Principal Beamline Scientist Dr Fred Mosselmans’ current research interests include the cycling of toxic metals by earthworms, the absorption of metals on bacterial cells and using synchrotron radiation to characterise and thereby help preserve historical materials. The Fischer Group has been at the leading edge of materials analysis, coating thickness measurement and micro hardness-testing technology for over 50 years. For more details on Fischer’s x-ray spectrometer s

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