Determination of Sulphur in organic and inorganic compounds

The oxygen flask method for the determination of sulphur in organic and inorganic compounds consists of a combustion procedure followed by a titrimetric determination. Combustion of the sample in oxygen yields water-soluble inorganic products, Percentage sulphur is determined by titration with Barium Perchlorate using Thorin screened with methylene blue indicator. Sulphur analysis in the presence of Phosphorus is not recommended...

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